Modification and development of the optical, structural, thermal and electrical characterization of Chitosan incorporated with Au/Bi2O3/Mo NPs fabricated by laser ablation

Rami Adel Pashameah; Hala A. Ibrahium; Nasser S. Awwad; M. O. Farea; Hoda A. Ahmed; M. A. El-Morsy; A. A. Menazea

doi:10.1007/s10904-022-02305-0

Modification and development of the optical, structural, thermal and electrical characterization of Chitosan incorporated with Au/Bi2O3/Mo NPs fabricated by laser ablation

Rami Adel Pashameah
, Hala A. Ibrahium
, Nasser S. Awwad
, M. O. Farea
, Hoda A. Ahmed
, M. A. El-Morsy
, A. A. Menazea

Physics

Research output: Contribution to journal › Article › peer-review

14 Scopus citations

Abstract

The molecular structures of pure polymer (chitosan) incorporated with ternary metal nanoparticles (Au/Bi₂O₃/Mo) synthesized by laser ablation have been performed ia FT-IR and XRD. The surface of the synthesized samples has been investigated ia SEM. Thermal, electrical, and dielectric haracterization have been performed to utilized in energy applications. XRD patterns display the amorphous nature of chitosan (Cs), characterized by two hump peaks at 2Ɵ =11.34^o and 2Ɵ =19.57^o, which disappeared by doped with Au/Bi₂O₃/Mo NPs. FT-IR spectra revealed that thereare complexation between Cs and Au/Bi₂O₃/Mo NPs took place in amorphous regions. SEM displays grains with rectangular shape after adding different filling nanoparticles, and rod-shaped formed on the surface of the samples.TGA curves obtained the enhancement in the thermal stability of samples. The AC conductivity of the samples increased by the addition of Au/Bi₂O₃/Mo NPs. The results confirm that nanocomposite of Cs/metal have excellent thermal and electronic haracterization, which may suggest the utilization of these nanocomposites in energy storage.

Original language	English
Pages (from-to)	2729-2736
Number of pages	8
Journal	Journal of Inorganic and Organometallic Polymers and Materials
Volume	32
Issue number	7
DOIs	https://doi.org/10.1007/s10904-022-02305-0
State	Published - Jul 2022

Keywords

AC conductivity
Chitosan
FT-IR
PLAL
TGA
XRD

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10.1007/s10904-022-02305-0

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Pashameah, R. A., Ibrahium, H. A., Awwad, N. S., Farea, M. O., Ahmed, H. A., El-Morsy, M. A., & Menazea, A. A. (2022). Modification and development of the optical, structural, thermal and electrical characterization of Chitosan incorporated with Au/Bi2O3/Mo NPs fabricated by laser ablation. Journal of Inorganic and Organometallic Polymers and Materials, 32(7), 2729-2736. https://doi.org/10.1007/s10904-022-02305-0

@article{ca7fe060639b454598ccae879164a3f3,

title = "Modification and development of the optical, structural, thermal and electrical characterization of Chitosan incorporated with Au/Bi2O3/Mo NPs fabricated by laser ablation",

abstract = "The molecular structures of pure polymer (chitosan) incorporated with ternary metal nanoparticles (Au/Bi2O3/Mo) synthesized by laser ablation have been performed ia FT-IR and XRD. The surface of the synthesized samples has been investigated ia SEM. Thermal, electrical, and dielectric haracterization have been performed to utilized in energy applications. XRD patterns display the amorphous nature of chitosan (Cs), characterized by two hump peaks at 2Ɵ =11.34o and 2Ɵ =19.57o, which disappeared by doped with Au/Bi2O3/Mo NPs. FT-IR spectra revealed that thereare complexation between Cs and Au/Bi2O3/Mo NPs took place in amorphous regions. SEM displays grains with rectangular shape after adding different filling nanoparticles, and rod-shaped formed on the surface of the samples.TGA curves obtained the enhancement in the thermal stability of samples. The AC conductivity of the samples increased by the addition of Au/Bi2O3/Mo NPs. The results confirm that nanocomposite of Cs/metal have excellent thermal and electronic haracterization, which may suggest the utilization of these nanocomposites in energy storage.",

keywords = "AC conductivity, Chitosan, FT-IR, PLAL, TGA, XRD",

author = "Pashameah, \{Rami Adel\} and Ibrahium, \{Hala A.\} and Awwad, \{Nasser S.\} and Farea, \{M. O.\} and Ahmed, \{Hoda A.\} and El-Morsy, \{M. A.\} and Menazea, \{A. A.\}",

note = "Publisher Copyright: {\textcopyright} 2022, The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature.",

year = "2022",

month = jul,

doi = "10.1007/s10904-022-02305-0",

language = "English",

volume = "32",

pages = "2729--2736",

journal = "Journal of Inorganic and Organometallic Polymers and Materials",

issn = "1574-1443",

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Pashameah, RA, Ibrahium, HA, Awwad, NS, Farea, MO, Ahmed, HA, El-Morsy, MA & Menazea, AA 2022, 'Modification and development of the optical, structural, thermal and electrical characterization of Chitosan incorporated with Au/Bi2O3/Mo NPs fabricated by laser ablation', Journal of Inorganic and Organometallic Polymers and Materials, vol. 32, no. 7, pp. 2729-2736. https://doi.org/10.1007/s10904-022-02305-0

Modification and development of the optical, structural, thermal and electrical characterization of Chitosan incorporated with Au/Bi2O3/Mo NPs fabricated by laser ablation. / Pashameah, Rami Adel; Ibrahium, Hala A.; Awwad, Nasser S. et al.
In: Journal of Inorganic and Organometallic Polymers and Materials, Vol. 32, No. 7, 07.2022, p. 2729-2736.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Modification and development of the optical, structural, thermal and electrical characterization of Chitosan incorporated with Au/Bi2O3/Mo NPs fabricated by laser ablation

AU - Pashameah, Rami Adel

AU - Ibrahium, Hala A.

AU - Awwad, Nasser S.

AU - Farea, M. O.

AU - Ahmed, Hoda A.

AU - El-Morsy, M. A.

AU - Menazea, A. A.

PY - 2022/7

Y1 - 2022/7

N2 - The molecular structures of pure polymer (chitosan) incorporated with ternary metal nanoparticles (Au/Bi2O3/Mo) synthesized by laser ablation have been performed ia FT-IR and XRD. The surface of the synthesized samples has been investigated ia SEM. Thermal, electrical, and dielectric haracterization have been performed to utilized in energy applications. XRD patterns display the amorphous nature of chitosan (Cs), characterized by two hump peaks at 2Ɵ =11.34o and 2Ɵ =19.57o, which disappeared by doped with Au/Bi2O3/Mo NPs. FT-IR spectra revealed that thereare complexation between Cs and Au/Bi2O3/Mo NPs took place in amorphous regions. SEM displays grains with rectangular shape after adding different filling nanoparticles, and rod-shaped formed on the surface of the samples.TGA curves obtained the enhancement in the thermal stability of samples. The AC conductivity of the samples increased by the addition of Au/Bi2O3/Mo NPs. The results confirm that nanocomposite of Cs/metal have excellent thermal and electronic haracterization, which may suggest the utilization of these nanocomposites in energy storage.

AB - The molecular structures of pure polymer (chitosan) incorporated with ternary metal nanoparticles (Au/Bi2O3/Mo) synthesized by laser ablation have been performed ia FT-IR and XRD. The surface of the synthesized samples has been investigated ia SEM. Thermal, electrical, and dielectric haracterization have been performed to utilized in energy applications. XRD patterns display the amorphous nature of chitosan (Cs), characterized by two hump peaks at 2Ɵ =11.34o and 2Ɵ =19.57o, which disappeared by doped with Au/Bi2O3/Mo NPs. FT-IR spectra revealed that thereare complexation between Cs and Au/Bi2O3/Mo NPs took place in amorphous regions. SEM displays grains with rectangular shape after adding different filling nanoparticles, and rod-shaped formed on the surface of the samples.TGA curves obtained the enhancement in the thermal stability of samples. The AC conductivity of the samples increased by the addition of Au/Bi2O3/Mo NPs. The results confirm that nanocomposite of Cs/metal have excellent thermal and electronic haracterization, which may suggest the utilization of these nanocomposites in energy storage.

KW - AC conductivity

KW - Chitosan

KW - FT-IR

KW - PLAL

KW - TGA

KW - XRD

UR - https://www.scopus.com/pages/publications/85129311288

U2 - 10.1007/s10904-022-02305-0

DO - 10.1007/s10904-022-02305-0

M3 - Article

AN - SCOPUS:85129311288

SN - 1574-1443

VL - 32

SP - 2729

EP - 2736

JO - Journal of Inorganic and Organometallic Polymers and Materials

JF - Journal of Inorganic and Organometallic Polymers and Materials

IS - 7

ER -

Pashameah RA, Ibrahium HA, Awwad NS, Farea MO, Ahmed HA, El-Morsy MA et al. Modification and development of the optical, structural, thermal and electrical characterization of Chitosan incorporated with Au/Bi2O3/Mo NPs fabricated by laser ablation. Journal of Inorganic and Organometallic Polymers and Materials. 2022 Jul;32(7):2729-2736. doi: 10.1007/s10904-022-02305-0

Modification and development of the optical, structural, thermal and electrical characterization of Chitosan incorporated with Au/Bi2O3/Mo NPs fabricated by laser ablation

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Keywords

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