Homogeneous deposition precipitation method for synthesis of carbon nanofibre based Cu-ZrO2 catalyst for hydrogenation of CO2 to methanol

Israf Ud Din; Maizatul S. Shaharun; Duvvuri Subbarao; A. Naeem

doi:10.4028/www.scientific.net/AMM.446-447.83

Homogeneous deposition precipitation method for synthesis of carbon nanofibre based Cu-ZrO₂ catalyst for hydrogenation of CO₂ to methanol

Israf Ud Din
, Maizatul S. Shaharun
, Duvvuri Subbarao
, A. Naeem

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

12 Scopus citations

Abstract

Deposition precipitation method was employed to synthesize carbon nanofiber based Cu-ZrO₂ catalyst (Cu-ZrO₂/CNF). Carbon nanofibre of herringbone type was used as a catalyst support. Prior deposition of catalyst particles, carbon nanofibre was oxidized to (CNF-O) with nitric acid solution. Catalyst was characterized by X-ray diffraction (XRD), Fourier Transmission Infrared (FTIR), Transmission Electron Microscopy (TEM) and Temperature-Programmed Reduction (TPR). Highly loaded, well-dispersed and thermally stable catalyst particles with average size of 4 nm were obtained by deposition precipitation method. Reaction studies confirmed the activity of the catalyst towards methanol formation.

Original language	English
Title of host publication	Advanced Research in Material Science and Mechanical Engineering
Pages	83-87
Number of pages	5
DOIs	https://doi.org/10.4028/www.scientific.net/AMM.446-447.83
State	Published - 2014
Externally published	Yes
Event	2013 2nd International Conference on Mechanics and Control Engineering, ICMCE 2013 - Beijing, China Duration: 1 Sep 2013 → 2 Sep 2013

Publication series

Name	Applied Mechanics and Materials
Volume	446-447
ISSN (Print)	1660-9336
ISSN (Electronic)	1662-7482

Conference

Conference	2013 2nd International Conference on Mechanics and Control Engineering, ICMCE 2013
Country/Territory	China
City	Beijing
Period	1/09/13 → 2/09/13

UN SDGs

This output contributes to the following UN Sustainable Development Goals (SDGs)

SDG 13 Climate Action

Keywords

Carbon nanofibers
Copper
Deposition precipitation
Zirconia

Access to Document

10.4028/www.scientific.net/AMM.446-447.83

Cite this

Ud Din, I., Shaharun, M. S., Subbarao, D., & Naeem, A. (2014). Homogeneous deposition precipitation method for synthesis of carbon nanofibre based Cu-ZrO₂ catalyst for hydrogenation of CO₂ to methanol. In Advanced Research in Material Science and Mechanical Engineering (pp. 83-87). (Applied Mechanics and Materials; Vol. 446-447). https://doi.org/10.4028/www.scientific.net/AMM.446-447.83

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title = "Homogeneous deposition precipitation method for synthesis of carbon nanofibre based Cu-ZrO2 catalyst for hydrogenation of CO2 to methanol",

abstract = "Deposition precipitation method was employed to synthesize carbon nanofiber based Cu-ZrO2 catalyst (Cu-ZrO2/CNF). Carbon nanofibre of herringbone type was used as a catalyst support. Prior deposition of catalyst particles, carbon nanofibre was oxidized to (CNF-O) with nitric acid solution. Catalyst was characterized by X-ray diffraction (XRD), Fourier Transmission Infrared (FTIR), Transmission Electron Microscopy (TEM) and Temperature-Programmed Reduction (TPR). Highly loaded, well-dispersed and thermally stable catalyst particles with average size of 4 nm were obtained by deposition precipitation method. Reaction studies confirmed the activity of the catalyst towards methanol formation.",

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author = "\{Ud Din\}, Israf and Shaharun, \{Maizatul S.\} and Duvvuri Subbarao and A. Naeem",

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Ud Din, I, Shaharun, MS, Subbarao, D & Naeem, A 2014, Homogeneous deposition precipitation method for synthesis of carbon nanofibre based Cu-ZrO₂ catalyst for hydrogenation of CO₂ to methanol. in Advanced Research in Material Science and Mechanical Engineering. Applied Mechanics and Materials, vol. 446-447, pp. 83-87, 2013 2nd International Conference on Mechanics and Control Engineering, ICMCE 2013, Beijing, China, 1/09/13. https://doi.org/10.4028/www.scientific.net/AMM.446-447.83

Homogeneous deposition precipitation method for synthesis of carbon nanofibre based Cu-ZrO₂ catalyst for hydrogenation of CO₂ to methanol. / Ud Din, Israf; Shaharun, Maizatul S.; Subbarao, Duvvuri et al.
Advanced Research in Material Science and Mechanical Engineering. 2014. p. 83-87 (Applied Mechanics and Materials; Vol. 446-447).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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AB - Deposition precipitation method was employed to synthesize carbon nanofiber based Cu-ZrO2 catalyst (Cu-ZrO2/CNF). Carbon nanofibre of herringbone type was used as a catalyst support. Prior deposition of catalyst particles, carbon nanofibre was oxidized to (CNF-O) with nitric acid solution. Catalyst was characterized by X-ray diffraction (XRD), Fourier Transmission Infrared (FTIR), Transmission Electron Microscopy (TEM) and Temperature-Programmed Reduction (TPR). Highly loaded, well-dispersed and thermally stable catalyst particles with average size of 4 nm were obtained by deposition precipitation method. Reaction studies confirmed the activity of the catalyst towards methanol formation.

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