TY - JOUR
T1 - Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane
AU - Alshammari, Mohammed B.
AU - Aly, Ashraf A.
AU - Bräse, Stefan
AU - Nieger, Martin
AU - Abd El-Haleem, Lamiaa E.
N1 - Publisher Copyright:
© 2022 American Chemical Society. All rights reserved.
PY - 2022/4/19
Y1 - 2022/4/19
N2 - The strategies of the syntheses of various (thio)ureas, semicarbazides, thiosemicarbazides, thiazolidones, and oxadiazole derived from the [2.2]paracyclophane molecule are achieved starting with 4-(2.2]paracyclophanyl)isocyanate. The structures of the obtained products were elucidated by NMR, mass spectrometry, and infrared (IR) spectroscopy in addition to high-resolution mass spectrometry (HRMS). X-ray structure analysis was also used to prove the assigned structure.
AB - The strategies of the syntheses of various (thio)ureas, semicarbazides, thiosemicarbazides, thiazolidones, and oxadiazole derived from the [2.2]paracyclophane molecule are achieved starting with 4-(2.2]paracyclophanyl)isocyanate. The structures of the obtained products were elucidated by NMR, mass spectrometry, and infrared (IR) spectroscopy in addition to high-resolution mass spectrometry (HRMS). X-ray structure analysis was also used to prove the assigned structure.
UR - http://www.scopus.com/inward/record.url?scp=85128535653&partnerID=8YFLogxK
U2 - 10.1021/acsomega.2c00141
DO - 10.1021/acsomega.2c00141
M3 - Article
AN - SCOPUS:85128535653
SN - 2470-1343
VL - 7
SP - 12879
EP - 12890
JO - ACS Omega
JF - ACS Omega
IS - 15
ER -