Decomposition-adsorption-deposition: An effective and novel technique for synthesis of hexagonal boron nitride microsheets

Pervaiz Ahmada; Mayeen Uddin Khandaker; Nawshad Muhammad; Iftikhar Ahmad; M. Abdul Rauf Khan; Ayaz Arif Khan; Ghulamullah Khan; Amir Sada Khan; Zahoor Ullah; Fida Rehman; Syed Muzamil Ahmed; Hazrat Ali; Muhammad Abdur Rehman; Mubashar Gulzar; Javed Iqbal; Syed Tawab Shah; Sohail Ahmed; Muhammad Shafiq

doi:10.1016/j.mssp.2018.08.002

Decomposition-adsorption-deposition: An effective and novel technique for synthesis of hexagonal boron nitride microsheets

Pervaiz Ahmada
, Mayeen Uddin Khandaker
, Nawshad Muhammad
, Iftikhar Ahmad
, M. Abdul Rauf Khan
, Ayaz Arif Khan
, Ghulamullah Khan
, Amir Sada Khan
, Zahoor Ullah
, Fida Rehman
, Syed Muzamil Ahmed
, Hazrat Ali
, Muhammad Abdur Rehman
, Mubashar Gulzar
, Javed Iqbal
, Syed Tawab Shah
, Sohail Ahmed
, Muhammad Shafiq

Research output: Contribution to journal › Article › peer-review

1 Scopus citations

Abstract

Magnesium diboride as a precursor with dual role of Nitrogen introduces a simple "decomposition-adsorption-deposition (DAD)" technique for the synthesis of Hexagonal Boron nitride microsheets (BNMSs) on silicon (Si) substrate at 1100 degrees C. The synthesized BNMSs has the apparent morphology like the white dispersed feathers on a plate surface with diameter in the range of 3-15 mu m and lengt greater than 30 mu m. All the BNMSs has the characteristics of h-BN lattice with an interlayer spacing of 0.34 nm. Boron and Nitrogen elemental compositions and h-BN phase of the synthesized BNMSs are verified from its characterization by X-ray photoelectron spectroscopy (XPS), Fourier transformed infrared (FTIR) spectroscopy and Raman.

Original language	English
Pages (from-to)	161-166
Number of pages	6
Journal	Materials Science in Semiconductor Processing
Volume	88
DOIs	https://doi.org/10.1016/j.mssp.2018.08.002
State	Published - Dec 2018
Externally published	Yes

Keywords

Microsheets
Reaction atmosphere
Synthesis
h-BN

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10.1016/j.mssp.2018.08.002

Cite this

Ahmada, P., Khandaker, M. U., Muhammad, N., Ahmad, I., Khan, M. A. R., Khan, A. A., Khan, G., Khan, A. S., Ullah, Z., Rehman, F., Ahmed, S. M., Ali, H., Rehman, M. A., Gulzar, M., Iqbal, J., Shah, S. T., Ahmed, S., & Shafiq, M. (2018). Decomposition-adsorption-deposition: An effective and novel technique for synthesis of hexagonal boron nitride microsheets. Materials Science in Semiconductor Processing, 88, 161-166. https://doi.org/10.1016/j.mssp.2018.08.002

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title = "Decomposition-adsorption-deposition: An effective and novel technique for synthesis of hexagonal boron nitride microsheets",

abstract = "Magnesium diboride as a precursor with dual role of Nitrogen introduces a simple {"}decomposition-adsorption-deposition (DAD){"} technique for the synthesis of Hexagonal Boron nitride microsheets (BNMSs) on silicon (Si) substrate at 1100 degrees C. The synthesized BNMSs has the apparent morphology like the white dispersed feathers on a plate surface with diameter in the range of 3-15 mu m and lengt greater than 30 mu m. All the BNMSs has the characteristics of h-BN lattice with an interlayer spacing of 0.34 nm. Boron and Nitrogen elemental compositions and h-BN phase of the synthesized BNMSs are verified from its characterization by X-ray photoelectron spectroscopy (XPS), Fourier transformed infrared (FTIR) spectroscopy and Raman.",

keywords = "Microsheets, Reaction atmosphere, Synthesis, h-BN",

author = "Pervaiz Ahmada and Khandaker, \{Mayeen Uddin\} and Nawshad Muhammad and Iftikhar Ahmad and Khan, \{M. Abdul Rauf\} and Khan, \{Ayaz Arif\} and Ghulamullah Khan and Khan, \{Amir Sada\} and Zahoor Ullah and Fida Rehman and Ahmed, \{Syed Muzamil\} and Hazrat Ali and Rehman, \{Muhammad Abdur\} and Mubashar Gulzar and Javed Iqbal and Shah, \{Syed Tawab\} and Sohail Ahmed and Muhammad Shafiq",

year = "2018",

month = dec,

doi = "10.1016/j.mssp.2018.08.002",

language = "English",

volume = "88",

pages = "161--166",

journal = "Materials Science in Semiconductor Processing",

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Ahmada, P, Khandaker, MU, Muhammad, N, Ahmad, I, Khan, MAR, Khan, AA, Khan, G, Khan, AS, Ullah, Z, Rehman, F, Ahmed, SM, Ali, H, Rehman, MA, Gulzar, M, Iqbal, J, Shah, ST, Ahmed, S & Shafiq, M 2018, 'Decomposition-adsorption-deposition: An effective and novel technique for synthesis of hexagonal boron nitride microsheets', Materials Science in Semiconductor Processing, vol. 88, pp. 161-166. https://doi.org/10.1016/j.mssp.2018.08.002

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T1 - Decomposition-adsorption-deposition

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AU - Ahmada, Pervaiz

AU - Khandaker, Mayeen Uddin

AU - Muhammad, Nawshad

AU - Ahmad, Iftikhar

AU - Khan, M. Abdul Rauf

AU - Khan, Ayaz Arif

AU - Khan, Ghulamullah

AU - Khan, Amir Sada

AU - Ullah, Zahoor

AU - Rehman, Fida

AU - Ahmed, Syed Muzamil

AU - Ali, Hazrat

AU - Rehman, Muhammad Abdur

AU - Gulzar, Mubashar

AU - Iqbal, Javed

AU - Shah, Syed Tawab

AU - Ahmed, Sohail

AU - Shafiq, Muhammad

PY - 2018/12

Y1 - 2018/12

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AB - Magnesium diboride as a precursor with dual role of Nitrogen introduces a simple "decomposition-adsorption-deposition (DAD)" technique for the synthesis of Hexagonal Boron nitride microsheets (BNMSs) on silicon (Si) substrate at 1100 degrees C. The synthesized BNMSs has the apparent morphology like the white dispersed feathers on a plate surface with diameter in the range of 3-15 mu m and lengt greater than 30 mu m. All the BNMSs has the characteristics of h-BN lattice with an interlayer spacing of 0.34 nm. Boron and Nitrogen elemental compositions and h-BN phase of the synthesized BNMSs are verified from its characterization by X-ray photoelectron spectroscopy (XPS), Fourier transformed infrared (FTIR) spectroscopy and Raman.

KW - Microsheets

KW - Reaction atmosphere

KW - Synthesis

KW - h-BN

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JO - Materials Science in Semiconductor Processing

JF - Materials Science in Semiconductor Processing

ER -

Decomposition-adsorption-deposition: An effective and novel technique for synthesis of hexagonal boron nitride microsheets

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Keywords

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